Contact an Account ManagerMass spectral characterization of urinary pipamperone metabolites and HPLC assay for pipamperone plasma levels
Summary
Type: HPLC
Application #: 104430
Catalog#: 720002.40 - MN HPLC Column, Nucleosil C18, 100A, 5um, 4x125mm
Detection: UV, 245nm
Conditions: eluent: 24:76 (v/v) mixture of acetonitrile and 5mM heptanesulphonic acid in water - 85% orthophosphoric acid (1000:0.86, v/v) adjusted to pH 3 with 0.1M NaOH
flow rate 1.5ml/min
Authors: Köppel C
Source: J Chromatogr 491 (1989) 432 - 438
Details
Legend: Fig. 4. Blank plasma sample (left) and plasma sample of a patient with a
pipamperone level of 25ng/ml (right). The pipamperone retention time of 7.82min
is indicated by arrows.